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1、Designation:D2171D2171M?10StardTestMethodfViscosityofAsphaltsbyVacuumCapillaryViscometer1ThisstardisissuedunderthefixeddesignationD2171D2171Mthenumberimmediatelyfollowingthedesignationindicatestheyearofiginaladoptioninth
2、ecaseofrevisiontheyearoflastrevision.Anumberinparenthesesindicatestheyearoflastreapproval.Asuperepsilon()indicatesaneditialchangesincethelastrevisionreapproval.ThisstardhasbeenapprovedfusebyagenciesoftheU.S.DepartmentofD
3、efense.Thistestmethodhasbeenapprovedbythesponsingcommitteesacceptedbythecooperatingsocietiesinaccdancewithestablishedprocedures.1.Scope1.1Thistestmethodcoversproceduresfthedeterminationofviscosityofasphaltbinder(bitumen)
4、byvacuumcapillaryviscometersat60C[140F].Itisapplicabletomaterialshavingviscositiesintherangefrom0.0036toover20000Pas[0.036toover200000P].NOTE1—Thistestmethodissuitablefuseatothertemperaturesbuttheprecisionisbasedondeterm
5、inationsonasphaltbindersat60C[140F].1.2ThevaluesstatedineitherSIunitsinchpoundunitsaretoberegardedseparatelyasstard.Thevaluesstatedineachsystemmaynotbeexactequivalentstherefeeachsystemshallbeusedindependentlyoftheother.C
6、ombiningvaluesfromthetwosystemsmayresultinnonconfmancewiththestard.1.3Warning—MercuryhasbeendesignatedbytheUnitedStatesEnvironmentalProtectionAgency(EPA)manystateagenciesasahazardousmaterialthatcancausecentralnervoussyst
7、emkidneyliverdamage.Mercuryitsvapmaybehazardoustohealthcrosivetomaterials.Cautionshouldbetakenwhenhlingmercurymercurycontainingproducts.SeetheapplicableproductMaterialSafetyDataSheet(MSDS)fdetailsEPA’swebsite—:www.epa.go
8、vmercuryfaq.htm—fadditionalinfmation.Usersshouldbeawarethatsellingmercurymercurycontainingproductsbothintoyourstatemaybeprohibitedbystatelaw.1.4Thisstarddoesnotpurpttoaddressallofthesafetyconcernsifanyassociatedwithitsus
9、e.Itistheresponsibilityoftheuserofthisstardtoestablishappropriatesafetyhealthpracticesdeterminetheapplicabilityofregulatylimitationspritouse.2.ReferencedDocuments2.1ASTMStards:2E1SpecificationfASTMLiquidinGlassThermomete
10、rsE11SpecificationfWovenWireTestSieveClothTestSievesE77TestMethodfInspectionVerificationofThermometers3.Terminology3.1Definitions:3.1.1Newtonianliquid—aliquidinwhichtherateofshearisproptionaltotheshearingstress.Theconsta
11、ntratiooftheshearingstresstotherateofshearistheviscosityoftheliquid.IftheratioisnotconstanttheliquidisnonNewtonian.3.1.2viscosity—theratiobetweentheappliedshearstressrateofsheariscalledthecoefficientofviscosity.Thiscoeff
12、icientisthusameasureoftheresistancetoflowoftheliquid.Itiscommonlycalledtheviscosityoftheliquid.TheSIunitofviscosityis1Pas(1Nsm2)iscalledaPalsecond.Thecgsunitofviscosityis1gcms(1dynescm2)iscalledapoise(P).1Pasisequivalent
13、to10P.4.SummaryofTestMethod4.1Thetimeismeasuredfafixedvolumeoftheliquidtobedrawnupthroughacapillarytubebymeansofvacuumundercloselycontrolledconditionsofvacuumtemperature.TheviscosityinPalsecondsiscalculatedbymultiplyingt
14、heflowtimeinsecondsbytheviscometercalibrationfact.NOTE2—Therateofsheardecreasesastheliquidmovesupthetubeitcanalsobevariedbytheuseofdifferentvacuumdifferentsizeviscometers.Thusthismethodissuitablefthemeasurementofviscosit
15、iesofNewtonian(simple)nonNewtonian(complex)liquids.1ThistestmethodisunderthejurisdictionofASTMCommitteeD04onRoadPavingMaterialsisthedirectresponsibilityofSubcommitteeD04.44onRheologicalTests.IntheIPthistestmethodisundert
16、hejurisdictionoftheStardizationCommittee.CurrenteditionapprovedJune12010.PublishedAugust2010.iginallyapprovedin1963.Lastpreviouseditionapprovedin2007asD2171–07ε1.DOI:10.1520D217110.2FreferencedASTMstardsvisittheASTMwebsi
17、tewww.astm.gcontactASTMCustomerServiceat.FAnnualBookofASTMStardsvolumeinfmationrefertothestard’sDocumentSummarypageontheASTMwebsite.Copyright?ASTMInternational100BarrHarbDrivePOBoxC700WestConshohockenPA194282959.UnitedSt
18、ates16.5.1.1Alternatingcurrentsthefrequenciesofwhichareintermittentlynotcontinuouslycontrolledasprovidedbysomepublicpowersystemscancauselargeerrsparticularlyovershttimingintervalswhenusedtoactuateelectricaltimingdevices.
19、7.SamplePreparations7.1Heatthesamplewithcaretopreventlocaloverheatinguntilithasbecomesufficientlyfluidtopouroccasionallystirringthesampletoaidheattransfertoassureunifmity.7.2Transferaminimumof20mLintoasuitablecontainerhe
20、atto13565.5C[275610F]stirringoccasionallytopreventlocaloverheatingtakingcaretoavoidtheentrapmentofair.NOTE4—Ifitissuspectedthatthesamplemaycontainsolidmaterialstrainthemeltedsampleintothecontainerthrougha300m[No.50]sieve
21、confmingtoSpecificationE11.NOTE5—Inthecaseofveryviscousmodifiedasphaltsitmaybenecessarytoheatinanovenat16365C[325610F]inderfthematerialtobecomesufficientlyfluidtostirpour.8.Procedure8.1Thespecificdetailsofoperationvaryso
22、mewhatfthevarioustypesofviscometers.SeethedetaileddeionsofviscometersinAppendixX1–AppendixX3finstructionsfusingthetypeofviscometered.Inallcaseshoweverfollowthegeneralproceduredescribedin8.1.1–8.1.9.8.1.1Maintainthebathat
23、thetesttemperaturewithin60.03C[0.05F].Applythenecessarycrectionsifanytoallthermometerreadings.8.1.2acleandryviscometerthatwillgiveaflowtimegreaterthan60spreheatto13565.5C[275610F].8.1.3getheviscometerbypouringtheprepared
24、sampletowithin62mmoffilllineE(Fig.2Fig.3Fig.4).8.1.4Placethegedviscometerinanovenbathmaintainedat13565.5C[275610F]faperiodof1062mintoallowlargeairbubblestoescape.8.1.5Removetheviscometerfromtheovenbathwithin5mintheviscom
25、eterinaholderpositiontheviscometerverticallyinthebathsothattheuppermosttimingmarkisatleast20mmbelowthesurfaceofthebathliquid.8.1.6Establisha40.060.07kPa[30060.5mmHg]vacuumbelowatmosphericpressureinthevacuumsystemconnectt
26、hevacuumsystemtotheviscometerwiththetogglevalvestopcockclosedinthelineleadingtotheviscometer.8.1.7Aftertheviscometerhasbeeninthebathf3065minstarttheflowofasphaltintheviscometerbyopeningthetogglevalvestopcockinthelinelead
27、ingtothevacuumsystem.8.1.8Measuretowithin0.1sthetimerequiredftheleadingedgeofthemeniscustopassbetweensuccessivepairsoftimingmarks.Reptthefirstflowtimewhichexceeds60sbetweenapairoftimingmarksnotingtheidentificationofthepa
28、iroftimingmarks.8.1.9Uponcompletionofthetestcleantheviscometerthoughlybyseveralrinsingswithanappropriatesolventcompletelymisciblewiththesamplefollowedbyacompletelyvolatilesolvent.Drythetubebypassingaslowstreamoffilteredd
29、ryairthroughthecapillaryf2minuntilthelasttraceofsolventisremoved.Alternativelytheviscometermaybecleanedinaglasscleaningovenatatemperaturenottoexceed500C[932F]followedbyrinseswithdistilleddeionizedwaterresiduefreeacetonef
30、iltereddryair.Periodicallyifdepositsareobservedcleantheinstrumentwithastrongacidcleaningsolutiontoremoveganicdepositsrinsethoughlywithdistilleddeionizedwaterresiduefreeacetonedrywithfiltereddryair.8.1.9.1Chromicacidclean
31、ingsolutionmaybepreparedbyaddingwiththeusualprecautions800mLofconcentratedsulphuricacidtoasolutionof92gofsodiumdichromatein458mLofwater.Theuseofsimilarcommerciallyavailablesulphuricacidcleaningsolutionsisacceptable.Nonch
32、romiumcontainingstronglyoxidizingacidcleaningsolutionsmaybesubstitutedsoastoavoidthedisposalproblemsofchromiumcontainingsolutions.8.1.9.2Useofalkalineglasscleaningsolutionsmayresultinachangeofviscometercalibrationisnotre
33、commended.9.Calculation9.1thecalibrationfactthatcrespondstothepairoftimingmarksusedfthedeterminationasprescribedin8.1.8.Calculaterepttheviscositytothreesignificantfiguresusingthefollowingequation:ViscosityPas5~Kt!(1)wher
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