超聲波-微波輔助離子液體催化脂肪酸甲酯化研究.pdf

1、 Classification Number：TS202 Unit Code: 10389 Security Level： Student ID: 1130919015 Dissertation for Master’s Degree of Fujian Agriculture and

2、Forestry University Study on esterification of fatty using ionic liquid as catalyst acid with ultrasonic-microwave assisted Category: Engineering Discipline: Food science and engineering Sub-Discipline: Food

3、science Research Field: Food processing theory and application Postgraduate: Zhengguo Wu Adrvisor: Zexiang Lu Prof. 目錄 目錄 摘 要.......................................................................................

4、....................................I ABSTRACT ......................................................................................................................I 第一章 緒論 ..............................................

5、...................................................................... 1 1.1 脂肪酸甲酯研究背景 ................................................................................................... 1 1.1.1 國(guó)外脂肪酸甲酯研究進(jìn)展 ............

6、......................................................................... 1 1.1.2 國(guó)內(nèi)脂肪酸甲酯研究現(xiàn)狀...................................................................................... 2 1.1.3 脂肪酸甲酯的制備方法 .....................

7、.................................................................... 3 1.2 離子液體的研究進(jìn)展 ................................................................................................... 5 1.2.1 離子液體的發(fā)展...................

8、................................................................................. 5 1.2.2 離子液體的分類.................................................................................................... 6 1.2.3 離子液體的合成方法.....

9、........................................................................................ 7 1.3 本論文的研究意義與主要內(nèi)容 ..................................................................................... 8 第二章 硫酸催化制備脂肪酸甲酯及工藝優(yōu)化 .

10、.................................................................. 9 2.1 引言 ........................................................................................................................... 9 2.2 材料與方法 .......

11、......................................................................................................... 9 2.2.1 實(shí)驗(yàn)材料與儀器 ..................................................................................................

12、. 9 2.2.2 實(shí)驗(yàn)方法............................................................................................................ 14 2.3 結(jié)果與討論 ...................................................................................

13、........................... 14 2.3.1 單因素實(shí)驗(yàn) ........................................................................................................ 14 2.3.2 響應(yīng)面法優(yōu)化酯化工藝.....................................................

14、.................................. 17 2.4 本章小結(jié) .................................................................................................................. 22 第三章 [PSMIM]HSO4 酸性離子液體催化制備脂肪酸甲酯及工藝優(yōu)化 .................

15、............ 23 3.1 引言 ......................................................................................................................... 23 3.2 材料與方法 .............................................................

16、.................................................. 23 3.2.1 材料與儀器......................................................................................................... 23 3.2.2 實(shí)驗(yàn)方法 ...................................

17、......................................................................... 24 3.3 結(jié)果與分析 ............................................................................................................... 24 3.3.1 酯化反應(yīng)影響因素的分析

18、.................................................................................... 24 3.3.2 響應(yīng)面法優(yōu)化脂肪酸甲酯制備工藝...................................................................... 27 3.4 本章小結(jié) ............................

19、...................................................................................... 32 第四章 超聲波-微波聯(lián)合輔助離子液體催化制備脂肪酸甲酯 ........................................... 33 4.1 引言 ................................................