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1、Designation:B244?09(Reapproved2014)EndsedbyAmericanElectroplaters’SocietyEndsedbyNationalAssociationofMetalFinishersStardTestMethodfMeasurementofThicknessofAnodicCoatingsonAluminumofOtherNonconductiveCoatingsonNonmagicBa
2、sisMetalswithEddyCurrentInstruments1ThisstardisissuedunderthefixeddesignationB244thenumberimmediatelyfollowingthedesignationindicatestheyearofiginaladoptioninthecaseofrevisiontheyearoflastrevision.Anumberinparenthesesind
3、icatestheyearoflastreapproval.Asuperepsilon()indicatesaneditialchangesincethelastrevisionreapproval.ThisstardhasbeenapprovedfusebyagenciesoftheU.S.DepartmentofDefense.1.Scope1.1Thistestmethodcoverstheuseofeddycurrentinst
4、rumentsfthenondestructivemeasurementofthethicknessofanonconductivecoatingonanonmagicbasismetal.Itisintendedtosupplementmanufacturers’instructionsftheoperationoftheinstrumentsisnotintendedtoreplacethem.1.2Thistestmethodis
5、particularlyusefulfmeasuringthethicknessofananodiccoatingonaluminumalloys.Chemicalconversioncoatingsaretoothintobemeasuredbythistestmethod.1.3ThevaluesstatedinSIunitsaretoberegardedasthestard.Thevaluesgiveninparenthesesa
6、refinfmationonly.1.4Thisstarddoesnotpurpttoaddressallofthesafetyconcernsifanyassociatedwithitsuse.Itistheresponsibilityoftheuserofthisstardtoestablishappropriatesafetyhealthpracticesdeterminetheapplicabilityofregulatylim
7、itationspritouse.2.ReferencedDocuments2.1ASTMStards:2B499TestMethodfMeasurementofCoatingThicknessesbytheMagicMethod:NonmagicCoatingsonMagicBasisMetals3.Terminology3.1DefinitionsofTermsSpecifictoThisStard:3.1.1accuracyn—t
8、hemeasureofthemagnitudeoferrbetweentheresultofameasurementthetruethicknessoftheitembeingmeasured.3.1.2adjustmentn—thephysicalactofaligningainstrument’sthicknessreadingstomatchthoseofaknownthicknesssample(removalofbias)in
9、dertoimprovetheaccuracyoftheinstrumentonaspecificsurfacewithinaspecificptionofitsmeasurementrange.Anadjustmentwillaffecttheoutcomeofsubsequentreadings.3.1.3calibrationn—thehighlevelcontrolleddocumentedprocessofobtainingm
10、easurementsontraceablecalibrationstardsoverthefulloperatingrangeoftheinstrumentthenmakingthenecessaryinstrumentadjustments(asrequired)tocrectanyoutoftoleranceconditions.3.1.3.1Discussion—Calibrationofcoatingthicknessinst
11、rumentsisperfmedbytheequipmentmanufactureranauthorizedagentbyanauthizedtrainedcalibrationlabatyinacontrolledenvironmentusingadocumentedprocess.Theoutcomeofthecalibrationprocessistoresterealigntheinstrumenttomeetexceedthe
12、manufacturer’sstatedaccuracy.3.1.4referencestardn—aspecimenofknownthicknessusedtoverifytheaccuracyofacoatingthicknessmeasuringinstrument.3.1.5verificationofaccuracyn—obtainingmeasurementsonareferencestardpritoinstrumentu
13、sefthepurposeofdeterminingtheabilityofthecoatingthicknessinstrumenttoproducereliablevaluescomparedtothecombinedinstrumentmanufacturer’sstatedaccuracythestatedaccuracyofthereferencestard.4.SummaryofTestMethod4.1Instrument
14、scomplyingwiththistestmethodmeasurecoatingthicknessbytheuseofeddycurrents.Aprobeisplaceddirectlyonthecoatedsurfaceinaperpendicularpositionelectroniccircuitryisusedtoconvertareferencesignalintoacoatingthicknessmeasurement
15、.1ThistestmethodisunderthejurisdictionofASTMCommitteeB08onMetallicInganicCoatingsisthedirectresponsibilityofSubcommitteeB08.10onTestMethods.CurrenteditionapprovedMay12014.PublishedMay2014.iginallyapprovedin1949.Lastprevi
16、ouseditionapprovedin2009asB244–09.DOI:10.1520B024409R14.2FreferencedASTMstardsvisittheASTMwebsitewww.astm.gcontactASTMCustomerServiceat.FAnnualBookofASTMStardsvolumeinfmationrefertothestard’sDocumentSummarypageontheASTMw
17、ebsite.Copyright?ASTMInternational100BarrHarbDrivePOBoxC700WestConshohockenPA194282959.UnitedStates18.5Curvature—Measurementsareaffectedbythecurvatureofthetestspecimen.Theinfluenceofcurvaturevariesconsiderablywiththemake
18、typeofinstrumentbutalwaysbecomesmepronouncedastheradiusofcurvaturedecreases.8.6SurfaceRoughness:8.6.11Measurementsareinfluencedbythesurfacetopographyofthesubstratethecoatingaroughsurfacewillgiveindividualinstrumentreadin
19、gsthatwillvaryfrompointtopoint.Inthiscaseitisnecessarytomakemanyreadingsatdifferentpositionstoobtainanaveragevaluethatisrepresentativeofthemeancoatingthickness.Ifthebasismetalisroughitmayalsobenecessarytocheckadjustifnec
20、essarythezerooftheinstrumentatseveralpositionsonasampleoftheuncoatedroughsubstrate.Iftheroughnessofthesubstratesurfaceissmallrelativetothecoatingthicknessitseffectwillprobablybenegligible.8.6.2Ifthebasismetalisroughitmay
21、alsobenecessarytocheckadjustifnecessarythezerooftheinstrumentatseveralpositionsonasampleoftheuncoatedroughsubstrate.Iftheroughnessofthesubstratesurfaceissmallrelativetothecoatingthicknessitseffectwillprobablybenegligible
22、.8.7FeignParticles—Theprobesofeddycurrentinstrumentsmustmakephysicalcontactwiththetestsurfacearetherefesensitivetofeignmaterialthatpreventsintimatecontactbetweentheprobethecoatingsurface.Boththetestsurfaceinstrumentprobe
23、shouldbekeptfreeoffeignmaterial.8.8Pressure—Thepressurewithwhichtheprobeisappliedtothetestspecimenaffectstheinstrumentreadingsshouldtherefebekeptconstant.8.9NumberofReadings—Theprecisionofthemeasurementscanbeimprovedbyin
24、creasingthenumberofreadingsinaccdancewithstatisticalprinciples.9.Procedure9.1Operateeachinstrumentinaccdancewiththeinstructionsofthemanufacturer.GiveappropriateattentiontothefactslistedinSection8.9.2Verifytheaccuracyofth
25、einstrumentatthetestsiteeachtimetheinstrumentisputintoserviceatfrequentintervalsduringusetoassureproperperfmance.9.3Manyinstrumentscanbeadjustedindertoimprovetheiraccuracyonaspecificsurfacewithinaspecificptionofitsmeasur
26、ementrange.Theeffectsofpropertiesofthesubstrate(compositionshaperoughnessedgeeffectselectricalproperties)coating(compositionmasssurfaceroughness)aswellasambientsurfacetemperaturesmayrequireadjustmentstobemadetotheinstrum
27、ent.Followthemanufacturer’sinstructions.9.4Observethefollowingprecautions:9.4.1BasisMetalThickness—Checkwhetherthebasismetalthicknessexceedsthecriticalthickness.Ifnoteitherusethebackupmethodin7.5makesurethatthecalibratio
28、nadjustmenthasbeenmadeonareferencestardhavingthesamethicknesselectricalpropertiesasthetestspecimen.9.4.2EdgeEffects—Donotmakereadingsclosetoanedgeholeinsidecneretc.ofaspecimenunlessthevalidityofthecalibrationadjustmentfs
29、uchameasurementhasbeendemonstrated.9.4.3Curvature—Donotmakereadingsonacurvedsurfaceofaspecimenunlessthevalidityofthecalibrationadjustmentfsuchameasurementhasbeendemonstrated.9.4.4NumberofReadings—Becauseofnmalinstrumentv
30、ariabilityitisnecessarytomakeseveralreadingsateachposition.Localvariationsincoatingthicknessmayalsorequirethatanumberofmeasurementsbemadeinanygivenareathisappliesparticularlytoaroughsurface(see8.9).9.4.5SurfaceCleanlines
31、s—Befemakingmeasurementscleananyfeignmattersuchasdirtgreasecrosionproductsfromthesurfacewithoutremovinganycoatingmaterial.10.Accuracy10.1Theinstrumentitscalibrationitsoperationshallbesuchthatthecoatingthicknesscanbedeter
32、minedwithin10%1mwhicheverisgreaterofthetruethickness.11.Rept11.1Thereptshallincludethefollowinginfmation:11.1.1Typeofinstrumentusedincludingmanufacturermodelnumberprincipleofoperationdateofcalibration11.1.2Sizedeionoftes
33、tspecimen11.1.3Whetherspecialjigswereused11.1.4Typeofcoatingthicknessstardreferencestardthemethodusedfaccuracyverificationanycalibrationadjustment11.1.5Thenumberofmeasurementstakenthevalueofeachmeasurement11.1.6Operatide
34、ntification11.1.7Date.NOTE1—Althoughtheeticallythistestmethodcanbeusedfmeasuringnonconductivecoatingsonamagicbasismetalitsusefcoatingsbelow25m(1mil)isnotrecommendedthemagicmethodoutlinedinTestMethodB499shallbeused.12.Pre
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