浙江科技學(xué)院本科生畢業(yè)論文

1、浙江科技學(xué)院本科生畢業(yè)論文1目錄1文獻(xiàn)綜述.........................................................................................................................................21.1國內(nèi)外生產(chǎn)概況及研究本課題的意義..........................................

2、......................................21.2本課題的目標(biāo)........................................................................................................................21.3反應(yīng)物介紹...........................................

3、..................................................................................21.3.1甲基三氯硅烷性質(zhì)...........................................................................................................21.3.2甲乙酮肟性質(zhì).....

4、.................................................................................................................41.3.3甲基三丁酮肟基硅烷性質(zhì)..........................................................................................

5、....41.3.4文獻(xiàn)合成方法簡介..........................................................................................................61.3.5溶劑的選擇.....................................................................................

6、.................................62實(shí)驗(yàn)部分.........................................................................................................................................82.1反應(yīng)原理....................................

7、............................................................................................82.2實(shí)驗(yàn)儀器及試劑....................................................................................................................8

8、2.2.1實(shí)驗(yàn)儀器..........................................................................................................................82.2.2實(shí)驗(yàn)試劑...............................................................................

9、...........................................82.3合成路線示意圖及裝置圖....................................................................................................82.3.1合成路線示意圖.................................................

10、.............................................................82.3.2合成裝置圖...........................................................................................................................92.4產(chǎn)品分析.................

11、..............................................................................................................113實(shí)驗(yàn)結(jié)果與討論....................................................................................................

12、.......................123.1原料的純化..........................................................................................................................123.2反應(yīng)影響因素的確定...................................................

13、.......................................................123.2.1甲乙酮肟與甲基三氯硅烷的摩爾比.............................................................................123.2.2不同溶劑的選擇....................................................

14、......................................................123.2.3反應(yīng)溫度的控制..........................................................................................................123.2.4反應(yīng)時(shí)間的選擇................................

15、..........................................................................133.3產(chǎn)品分離...............................................................................................................................133.3.1無溶劑

16、法.........................................................................................................................133.3.2加溶劑法.......................................................................................

17、..................................133.4甲基三丁酮肟基硅烷中少量甲乙酮肟的除去...................................................................143.5過量原料回收....................................................................................

18、..................................143.5.1基本原理........................................................................................................................143.5.2回收過程描述..........................................

19、......................................................................143.6實(shí)驗(yàn)結(jié)果匯總......................................................................................................................154結(jié)論與展望.............

20、......................................................................................................................18參考文獻(xiàn)................................................................................................

21、..........................................20致謝..........................................................................................................................................21附錄................................